[読みたい論文] 「生きている」ラジカル重合

Viewed: 05:02:00 in December 11, 2019

Posted: May 22, 2019

Synthesis of Poly(N-vinylamide)s and Poly(vinylamine)s and Their Block Copolymers by Organotellurium-Mediated Radical Polymerization (Fan, Weijia; Yamago, Shigeru)
Angew. Chem. Int. Ed. 2019, 58 (21), 7113−7116.

Keywords: TERP; NMVA; NVA; NVF; V-601


ビニルアミドの重合反応について報告しているようです。重合触媒(になるんだと思います)は、イソ酪酸メチルのα炭素にテルル原子が結合した化合物。上の反応式にはありませんが、重合開始剤としてV-601 (dimethyl 2,2'-azobis(isobutyrate))を使用しています。

重合末端とモノマーが反応してポリマーが長くなっていく過程で形式的にのテルル原子がモノマー分子の末端になっていく炭素に移動していくので、原子移動ラジカル重合(ATRP)と言ってもいいような気もしますが、論文の要旨にはテルル化合物によるラジカル重合とあります。テルル化合物であることを強調したかったのか、それとも他の理由なのか、論文のキモの部分のような気がしますので、読みたい論文に追加したいと思いました。

そしてこの重合、分散度が1.25未満ですし、得られたポリマーと他の種類のモノマーを反応させてブロック共重合体を得ることができますので、リビング重合と言って差し支えないのではと思ったりもするのですが…(最近はリビングかどうか判断する基準が厳しいのかもしれません)。

この記事を書いた人
「牧岡ふうふ堂」オーナー。博士(工学)。
酒都圏在住。
某地方の国立系工業大学でアシスタントをしていました。 専門は有機反応・金属錯体(主に希土類)・π共役系。
twitterアカウントは@makiokafufudo(お仕事用)、@ymakioka(個人用)です。

 

1984年はこんな年

人名反応など
Chan転位 [Doi 1]
Imamotoセリウム反応剤 [Doi 1]
Narasaka−Prasad還元 [Doi 1]
ノーベル化学賞
固相反応によるペプチド化学合成法の開発
(Robert Bruce Merrifield)
できごと
米アップルコンピュータがMacintoshを発表
「タカラ缶チューハイ」発売(宝酒造=宝ホールディングス)
植村直己がマッキンリー山の単独登頂に成功
「風の谷のナウシカ」公開
グリコ・森永事件
東京芝浦電気が東芝へ社名変更
プランタン銀座が開業
東洋工業がマツダへ社名変更
NHKが衛星放送を開始
第二電電(KDDI)設立
「8時だョ!全員集合」公開生放送中に停電
紙おむつ「メリーズ」発売(花王石鹸=花王)
「ビオレU」を発売(花王石鹸=花王)
投資ジャーナル事件
フィルムセンター火災
オーストラリアからコアラ
「北斗の拳」放映開始(フジテレビ)
住友製薬発足
新紙幣発行
「フライデー」創刊
キャプテンシステムのサービスを開始
エリマキトカゲ大流行
「名探偵ホームズ」放送開始

 

きょうのどうぶつ

ここの画像を使用しています。

JR西条駅で見かけた東広島市公認キャラクター「のん太」。

 

計算終わりました

 

あわせてどうぞ

SOHOのすすめ記事一覧 2019年
お仕事関係の記事のリストです(2019年)。

読みたい論文シリーズ − 2019年2Q
読みたいけと読んでいない論文を、構造式を描きながら紹介します(2019年4〜6月)。

 

[読みたい論文] マグネシウム触媒でアルキンのヒドロボリル化
金属単体でではないです。
Angew. Chem. Int. Ed. 2019, 58 (21), 7025−7029.

[読みたい論文] 名前を出すのに気を使ってしまう酢酸エステルのα-メチル化
メタノールがメチル源です。
Org. Lett. 2019, 21 (9), 3299−3303.

[読みたい論文] 交換反応でボロン酸エステルをフリーのボロン酸にします
ボロン酸を以ってボロン酸エステルを制す。
Org. Lett. 2019, 21 (9), 3048−3052.

[読みたい論文] 窒素を飛ばすとベンゼン環が飛びます
アジドとホウ素ルイス酸の反応。
Angew. Chem. Int. Ed. 2019, 58 (20), 6540−6544.

[読みたい論文] 欲求不満がさらに強まったルイスペア
より嵩高く、より強引に。
Angew. Chem. Int. Ed. 2019, 58 (20), 6737−6741.

[読みたい論文] 1級アルコールから始まる、Grignard反応剤を使わない直接的ケトン合成
フラスコの外から見れば直接合成です。
J. Am. Chem. Soc. 2019, 141 (17), 6869−6874.

[読みたい論文] ロジウム触媒下でのケトン合成: 配位子で作り分けます。
アルデヒドと臭化ビニル化合物から。
J. Am. Chem. Soc. 2019, 141 (17), 6864−6868.

[読みたい論文] アミドの反応性をNMRで予測します
じれねじれてケミカルシフト
Chem. Commun. 2019, 55 (30), 4423−4426.

[読みたい論文] テトラヒドロフランを2分子から立体選択的に作ります
チタンアルコキシドとフルオロアルキルアルコール下での分子間環化
J. Am. Chem. Soc. 2019, 141 (16), 6489−6493.

[読みたい論文] ビニルエーテルのSuzuki−Miyaura型アリール化
アルコキシル基が脱離します。
Org. Lett. 2019, 21 (8), 2913−2917.

 

注目のWebコンテンツ

クラウドファンディング:神戸大学の調査船
(海の研究者)
https://goto33.blog.so-net.ne....

他人の利益を考慮する意思決定の脳回路
(理化学研究所)
http://www.riken.jp/pr/press/2...

光を使って神経回路をトレースする
(理化学研究所)
http://www.riken.jp/pr/press/2...

ペースダウン
(ある女性研究者の日記)
https://sunnily.exblog.jp/3060...

森戸国際高等教育学院「ウェルカムデスク」を開設します ―留学生等が気軽に相談できる窓口を、民間との協力によるカフェに併設―
(広島大学)
https://www.hiroshima-u.ac.jp/...

今月のNature INDEX ピックアップ
(筑波大学)
http://www.tsukuba.ac.jp/news/...

 

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Structures and Photoluminescence of Silver(I) and Gold(I) Cyclic Trinuclear Complexes with Aryl Substituted Pyrazolates
(Saotome, Mai; Shimizu, Daichi; Itagaki, Ayaka; Young, David James; Fujisawa, Kiyoshi)
Tag: PL, SS, Naph, Nap, Np, CC, Ph, Ar

鉄  
[Chem. Lett. 20190521090237, 2019, 6−525]
Cis-1,4 Specific Polymerization of 1,3-Butadiene Using PNP-pincer Ligated Iron(II) Complexes
(Tanaka, Ryo; Ikeda, Kenshi; Nakayama, Yuushou; Shiono, Takeshi)
Tag: PBd, PBD, PB, Fe, MAO, HMW, pyr, BD, C4H6, Py, e-, C

層状複水酸化物 パラジウム  
[Chem. Lett. 20190521090250, 2019, 6−517]
Heterogeneously Palladium-catalyzed Acceptorless Dehydrogenative Aromatization of Cyclic Amines
(Oyama, Takashi; Yatabe, Takafumi; Jin, Xiongjie; Mizuno, Noritaka; Yamaguchi, Kazuya)
Tag: Pd, LDH, THIQ, NH2, pip, PIPD, LDH, C, Cat

イオン液体  
[Chem. Lett. 20190521090249, 2019, 6−521]
Catalytic Carbonization of Acenaphthene for the Preparation of Ordered Mesoporous Carbon CMK-1 toward Application as Electrochemical Double-layer Capacitor Electrode with Ionic Liquid Electrolyte
(Hirano, Yoko; Iba, Yoshiki; Kuroda, Naoto; Kubota, Yoshihiro; Inagaki, Satoshi)
Tag: OMC, EDL, C, EC, IL, EDLC, EDL, DLC, e-, Cat

[Chem. Lett. 2019052109032, 2019, 6−513]
Simulation of Conductive Atomic Force Microscopy of Organic Photovoltaics by Dynamic Monte Carlo Method
(Kawashima, Eisuke; Fujii, Mikiya; Yamashita, Koichi)
Tag: AF, PV, OPV, OVD, MC, cAFM, AFM, DMC

[Chem. Lett. 20190521090317, 2019, 6−506]
Synthesis of a Novel AB Block Copolyaceylene Consisting of a Dynamic Cis-transoidal Racemic Helical Sequence and a Static Cis-cisoidal One-handed Helical Sequence
(Yin, Guanwu; Suzuki, Junpei; Aoki, Toshiki; Teraguchi, Masahiro; Kaneko, Takashi)
Tag: BCP, M, DP

[Chem. Lett. 20190521090316, 2019, 6−510]
Cyclization Reaction of 4-Acyl-1-sulfonyl-1,2,3-triazoles Possessing Phenyl Rings through Generation of Electron-deficient Carbenoids
(Zhao, Qiang; Miura, Tomoya; Murakami, Masahiro)
Tag: Hvtz, CHB, C, Bn, TAZ, E, El, EAS, Ph, e-, Rh

[Chem. Lett. 20190521090319, 2019, 6−502]
Preparation of Nanoporous Silica Gel Using Oxidatively Degradable Polymer in Organic–Inorganic Hybrid
(Kudo, Eiichi; Kihara, Nobuhiro)
Tag: COOH, TEOS, SC

[Bull. Chem. Soc. Jpn 20190521090345, 2019, 6−1018]
Chemical Sensing of Acrolein-Amine Conjugates for Food Quality Control: A Case Study of Milk Products
(Kishimoto, Arisa; Nomura, Shogo; Tanaka, Katsunori)
Tag: For, AGE, 107-02-8, Lys, K, ACR, NH2, FG, FDP, QC