Viewed: 10:18:02 in January 25, 2020

Synthesis of α,β-Disubstituted Acrylates via Galat Reaction (Xavier, Tania; Condon, Sylvie; Pichon, Christophe; Le Gall, Erwan; Presset, Marc)
Org. Lett. 2019, 21 (15), 6135−6139.

Keywords: morpholine; 4-dimethylaminopyridine

モルホリン触媒下でのアルデヒドとマロン酸モノエステル(論文中ではハーフエステルと書いている)の脱炭酸縮合に関する論文のようです。生成物はα,β-不飽和カルボン酸エステル。「フリー」のマロン酸での検討はしていないっぽい。

反応自体はGraphical Abstractに示されている通りシンプルなのですが、Supporting Informationを読んで行くと酢酸やDMAPが入っていたりで、モルホリンの触媒としての力が若干弱いのかなと言う気もします。何より気になるのが「どう言う経緯でモルホリンを触媒として採用するに至ったのか」と言う点。何か別の反応を期待していたのかなあとか、類似の化合物を色々検討した結果なのかなとか思ったりもしてます。

要旨だけ見ていると、なんでこれがOrg. Lett.にアクセプトされたのかなあと、SynlettやTetrahedron Lett.とかの方がいいんじゃないかなあと思ったのですが、本文中にもっとインパクトがある記述があるかもしれないので、読みたい論文に追加です。

 

Asinger反応 [Doi 1]
Brownヒドロホウ素化 [Doi 1]
Doering−LaFlammeアレン合成 [Doi 1]
Lawesson試薬 [Doi 1]
Lemieux−Johnson酸化 [Doi 1]
気相系の化学反応速度論(特に連鎖反応)に関する研究
(Sir Cyril Norman Hinshelwood, Nikolay Nikolayevich Semyonov)
「自動車損害賠償保障法」(自賠責法)施行、自賠責保険の強制加入
「週刊新潮」創刊(新潮社)
日本で初の人工心肺を用いた開心術成功(大阪大学)
水俣病第一号患者公式確認
日本登山隊がマナスル初登頂に成功
気象庁発足(中央気象台から改称)
日本初の台所用洗剤「ライポンF」発売(ライオン油脂=ライオン株式会社)
第二種運転免許、大型自動車運転免許が施行
東急ストア設立
日ソ共同宣言
大阪の通天閣が再建
東京飲料(東京コカ・コーラボトリング)設立
日本初の漫画週刊誌「週刊漫画TIMES」創刊(芳文社)
日本が国際連合に加盟
IBMが世界初のハードディスクを発売(5MB)

 

ここの画像を使用しています。

空中を舞うアゲハ。

 

Just finished the calculations: 2-C-methyl-D-erythritol 4-phosphate (MEP) https://t.co/PiJ2VYrMgR pic.twitter.com/W4lQdCwiZg

— nanoniele (@nanoniele) August 5, 2019

 

　

 

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[Thin Solid Films 2019080209418, 2019, −299]
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Tag: PSD, MS, Abs, Hx, Hex, TF, IR

[Thin Solid Films 20190802094157, 2019, −210]
Structural and electrical properties of Sb-doped SnO2 thin films prepared by metal organic decomposition
(Sawahata, Junji; Kawasaki, Tasuku)
Tag: AF, pc, XR, MOD, XRD, AFM, TF

[Thin Solid Films 2019080209449, 2019, −180]
Porosity-tuned thermal conductivity in thermoelectric Al-doped ZnO thin films grown by mist-chemical vapor deposition
(Saini, Shrikant; Mele, Paolo; Oyake, Takafumi; Shiomi, Junichiro; Niemel�, Janne-Petteri; Karppinen, Maarit; Miyazaki, Koji; Li, Chaoyang; Kawaharamura, Toshiyuki; Ichinose, Ataru; Molina-Luna, Leopoldo)
Tag: PF, TC, PLD, FOM, CVD, TF

[J. Alloys Compd. 20190802094623, 2019, −1155]
Microstructure, mechanical properties, and damping capacity in stir zone after friction stir welding of Fe�?17Mn damping alloy
(Lee, Seung-Joon; Shin, Se Eun; Ushioda, Kohsaku; Fujii, Hidetoshi)
Tag: SF, UTS, SFE, TRIP, FSW

[J. Alloys Compd. 20190802094954, 2019, −901]
Grain refinement and superplastic flow in friction stir processed Ti�?15V�?3Cr�?3Sn�?3Al alloy
(Zhang, Wenjing; Liu, Huihong; Ding, Hua; Fujii, Hidetoshi)
Tag: GB, Ti, DRX, CDRX, FSP, HAGB

[J. Alloys Compd. 20190802095850, 2019, −678]
Niobium oxynitrides with defective rock salt-type structures
(Tateno, Kota; Masubuchi, Yuji; Kikkawa, Shinichi)
Tag: RS, N, Nb, SG

[Acta Biomater. 20190802101313, 2019, −183]
Differential outcomes of venous and arterial tissue engineered vascular grafts highlight the importance of coupling long-term implantation studies with computational modeling
(Best, Cameron A.; Szafron, Jason M.; Rocco, Kevin A.; Zbinden, Jacob; Dean, Ethan W.; Maxfield, Mark W.; Kurobe, Hirotsugu; Tara, Shuhei; Bagi, Paul S.; Udelsman, Brooks V.; Khosravi, Ramak; Yi, Tai; Shinoka, Toshiharu; Humphrey, Jay D.; Breuer, Christopher K.)
Tag: TE, L-Lac, EC, ML, CL, Mat, ECM, ESP

[Acta Biomater. 20190802101526, 2019, −320]
Hyaluronic acid hydrogels with defined crosslink density for the efficient enrichment of breast cancer stem cells
(Tan, Susi; Yamashita, Atsushi; Gao, Shu Jun; Kurisawa, Motoichi)
Tag: HA, TF, ALDH, BCC, CSC

[Acta Biomater. 20190802101526, 2019, −361]
Development of a collagen-like peptide polymer via end-to-end disulfide cross-linking and its application as a biomaterial
(Ichise, Shinichiro F.; Takeuchi, Shungo; Aoki, Shigehisa; Kuroda, Kazuki C.; Nose, Hiroshi; Masuda, Ryo; Koide, Takaki)
Tag: CLP, THP, COL, ETE

[Organometallics 20190802101921, 2019, 14−2701]
Structure of the Complex Ni(C₈H₁₂)(L) and Its Reactivity toward Organometallic Reagents
(Iwasaki, Takanori; Yokoyama, Wataru; Kambe, Nobuaki)
Tag: C, Al, DB, BD, C4H6

[Organometallics 20190802101922, 2019, 14−2705]
Formation of a Î�₃-Acetylide on a Ru₃ Cluster via Coupling of Î�-Methylene with Isocyanide Accompanied by Elimination of Amine: A Model of Hydrogen-Assisted C–C Bond Formation on a Metal Surface
(Chikamori, Hiroki; Takao, Toshiro)
Tag: Ru, H, NH2, PhSMe, e-

[Organometallics 20190802102136, 2019, 14−2834]
Iridium-Mediated Arylation of Quinoline via the Cleavage of Carbon–Carbon and Carbon–Nitrogen Bonds of 1,3-Dimesitylimidazol-2-ylidene
(Sakurai, Shun; Tobisu, Mamoru)
Tag: IMes, Ir, 91-22-5

[Organometallics 20190802102157, 2019, 14−2863]
Synthesis and Catalytic Reactivity of Bis(molybdenum-trihalide) Complexes Bridged by Ferrocene Skeleton toward Catalytic Nitrogen Fixation
(Itabashi, Takayuki; Arashiba, Kazuya; Tanaka, Hiromasa; Konomi, Asuka; Eizawa, Aya; Nakajima, Kazunari; Yoshizawa, Kazunari; Nishibayashi, Yoshiaki)
Tag: Mo, Fe, CV, CV, N, fc, e-, DFT, Cat

[Macromolecules 2019080210220, 2019, 14−5067]
Polymer Alloying of Helical Syndiotactic PMMA with [60]Fullerene-End-Capped Polymers through Inclusion Complex Formation of the Helical Cavity with Fullerene Units
(Kawauchi, Takehiro; Ohnishi, Keita; Kajihara, Kouta; Kawauchi, Mariko; Takeichi, Tsutomu)
Tag: C60, PhMe, PMMA, TolH, PDMS

[Macromolecules 20190802102223, 2019, 14−5086]
Dynamics of Critical Clusters Synthesized by End-Coupling of Four-Armed Poly(ethylene glycol)s
(Li, Xiang; Noritomi, Takako; Sakai, Takamasa; Gilbert, Elliot P.; Shibayama, Mitsuhiro)
Tag: DLS, LS, LDS, ALGM, as, PEG, DSL, FG, DLA, PE

[Macromolecules 20190802102244, 2019, 14−5110]
Phase Behavior of Grafted Polymer Nanocomposites from Field-Based Simulations
(Koski, Jason P.; Krook, Nadia M.; Ford, Jamie; Yahata, Yoshikazu; Ohno, Kohji; Murray, Christopher B.; Frischknecht, Amalie L.; Composto, Russell J.; Riggleman, Robert A.)
Tag: DP, LD, Mat, PN, PSt, PNC, PMMA, NP, PGN, PS, DOP

[Macromolecules 20190802102318, 2019, 14−5157]
“Structurally Neutral�? Densely Packed Homopolymer-Adsorbed Chains for Directed Self-Assembly of Block Copolymer Thin Films
(Morimitsu, Yuma; Salatto, Daniel; Jiang, Naisheng; Sen, Mani; Nishitsuji, Shotaro; Yavitt, Benjamin M.; Endoh, Maya K.; Subramanian, Ashwanth; Nam, Chang-Yong; Li, Ruipeng; Fukuto, Masafumi; Zhang, Yugang; Wiegart, Lutz; Fluerasu, Andrei; Tanaka, Keiji; Koga, Tadanori)
Tag: Lam, SC, PCS, Si, GI, GISAX, GISAXS, PSt, DBCP, PMMA, DSA, COSY, XPCS, SA, PS, TF, BCP

[Macromolecules 2019080210268, 2019, 14−5325]
Macromolecular [2]Rotaxanes Linked with Polystyrene: Properties and Nanoscale Film Morphologies
(, Brian; Ree, J.; Aoki, Daisuke; Kim, Jehan; Satoh, Toshifumi; Takata, Toshikazu; Ree, Moonhor)
Tag: GIXS, Lam, GI, PSt, DBCP, VL, PS

[Langmuir 20190802103145, 2019, 29−9611]
Adsorption and Capillary Condensation-Induced Imbibition in Nanoporous Media
(Cihan, Abdullah; Tokunaga, Tetsu K.; Birkholzer, Jens T.)
Tag: C, RH

[Langmuir 20190802103245, 2019, 28−9139]
Quick Liquid Propagation on a Linear Array of Micropillars
(Mu, Lizhong; Yoshikawa, Harunori N.; Zoueshtiagh, Farzam; Ogawa, Tetsuya; Motosuke, Masahiro; Ueno, Ichiro)
Tag: HE

[Langmuir 20190802103253, 2019, 28−9152]
Electrostatic Adsorption Behavior of Zwitterionic Copolymers on Negatively Charged Surfaces
(Wang, Sheng-Yao; Fang, Li-Feng; Matsuyama, Hideto)
Tag: CA, QCMB, QCM

[Langmuir 20190802103341, 2019, 28−9194]
Two-Dimensional Nonclose-Packed Colloidal Crystals by the Electrostatic Adsorption of Three-Dimensional Charged Colloidal Crystals
(Aoyama, Yurina; Toyotama, Akiko; Okuzono, Tohru; Yamanaka, Junpei)
Tag: CC, APTES, Au, PSt, APTEOS, APS, APTS, PS, PVF, SiH4

[Chem. Mater. 2019080210372, 2019, 14−5056]
Atomic Layer Deposition of Pt Thin Films Using Dimethyl (N,N-Dimethyl-3-Butene-1-Amine-N) Platinum and O₂ Reactant
(Lee, Woo-Jae; Wan, Zhixin; Kim, Chang-Min; Oh, Il-Kwon; Harada, Ryosuke; Suzuki, Kazuharu; Choi, Eun-Ae; Kwon, Se-Hun)
Tag: AR, ALD, Pt, NH2, Tdep, WF, TF, Cat

[Chem. Mater. 20190802103917, 2019, 14−5190]
Dense Charge Accumulation in MXene with a Hydrate-Melt Electrolyte
(Kim, Kijae; Ando, Yasunobu; Sugahara, Akira; Ko, Seongjae; Yamada, Yuki; Otani, Minoru; Okubo, Masashi; Yamada, Atsuo)
Tag: EC, Ti, Li, EES, ESD, ED

[Chem. Mater. 2019080210422, 2019, 14−5314]
Nickel Germanide Thin Films by Atomic Layer Deposition
(V�yrynen, Katja; Vihervaara, Anton; Hatanp��, Timo; Mattinen, Miika; Heikkil�, Mikko J.; Mizohata, Kenichiro; R�is�nen, Jyrki; Ritala, Mikko; Leskel�, Markku)
Tag: ALD, Ni, TF

[Polym. Chem. 20190802104241, 2019, 29−3951]
Synthesis of chain end acyl-functionalized polymers by living anionic polymerization: versatile precursors for H-shaped polymers
(Takahata, Kazuki; Uchida, Satoshi; Goseki, Raita; Ishizone, Takashi)
Tag: LAP

[New J. Chem. 2019080210457, 2019, 29−11477]
Catalytic methane oxidation by a supramolecular conjugate based on a �-nitrido-bridged iron porphyrinoid dimer
(Yamada, Yasuyuki; Morita, Kentaro; Mihara, Nozomi; Igawa, Kazunobu; Tomooka, Katsuhiko; Tanaka, Kentaro)
Tag: Fe, CH4, Cat

[New J. Chem. 20190802104823, 2019, 29−11643]
A reversible and turn-on type fluorescence behaviour of hydrogen sulfide via a redox cycle between selenoxide and selenide
(Annaka, Tatsuro; Nakata, Norio; Ishii, Akihiko)
Tag: FL, H, BD, C4H6, H2S

[New J. Chem. 20190802104935, 2019, 29−11720]
Preparation of zinc oxide with a three-dimensionally interconnected macroporous structure via a sol–gel method accompanied by phase separation
(Lu, Xuanming; Kanamori, Kazuyoshi; Nakanishi, Kazuki)
Tag: ZnO, Zn

[ACS Infect. Dis. 20190802105950, 2019, 7−1045]
IID572: A New Potentially Best-In-Class �-Lactamase Inhibitor
(Reck, Folkert; Bermingham, Alun; Blais, Johanne; Casarez, Anthony; Colvin, Richard; Dean, Charles R.; Furegati, Markus; Gamboa, Luis; Growcott, Ellena; Li, Cindy; Lopez, Sara; Metzger, Louis; Nocito, Sandro; Ossola, Flavio; Phizackerley, Kaci; Rasper, Dita; Shaul, Jacob; Shen, Xiaoyu; Simmons, Robert L.; Tang, Dazhi; Tashiro, Kyuto; Yue, Qin)

[ACS Infect. Dis. 20190802110130, 2019, 7−1177]
Inhibition of Biofilm Formation by Candida albicans and Polymicrobial Microorganisms by Nepodin via Hyphal-Growth Suppression
(Lee, Jin-Hyung; Kim, Yong-Guy; Khadke, Sagar Kiran; Yamano, Aki; Watanabe, Akio; Lee, Jintae)
Tag: SA, T

[ACS Earth Space Chem. 20190802110425, 2019, 7−1268]
Effects of Phase State and Phase Separation on Dimethylamine Uptake of Ammonium Sulfate and Ammonium Sulfate–Sucrose Mixed Particles
(, Wing-Sy; DeRieux, Wong; Chu, Yangxi; Chan, Chak K.; Glicker, Hayley S.; Smith, James N.; Zuend, Andreas; Shiraiwa, Manabu)
Tag: am, NH2, AS, 57-50-1, DMA, NP, NPF, RH

[ACS Earth Space Chem. 20190802110545, 2019, 7−1346]
Mussel Shell Geochemical Analyses Reflect Coastal Environmental Changes Following the 2011 Tohoku Tsunami
(Murakami-Sugihara, Naoko; Shirai, Kotaro; Hori, Masako; Amano, Yosuke; Fukuda, Hideki; Obata, Hajime; Tanaka, Kiyoshi; Mizukawa, Kaoruko; Sano, Yuji; Takada, Hideshige; Ogawa, Hiroshi)
Tag: em

[ACS Appl. Energy Mater. 20190802111623, 2019, 7−4597]
Ligand-Effect-Induced Oxygen Reduction Reaction Activity Enhancement for Pt/Zr/Pt(111) Surfaces with Tensile Strain Relieved by Stacking Faults
(Kudo, Daisuke; Kaneko, Soma; Myochi, Rikiya; Chida, Yoshihiro; Todoroki, Naoto; Tanabe, Tadao; Wadayama, Toshimasa)
Tag: SF, APD, EC, CT, O, ORR

[ACS Appl. Energy Mater. 20190802112036, 2019, 7−4801]
Examining the Role of Anisotropic Morphology: Comparison of Free-Standing Magnetite Nanorods versus Spherical Magnetite Nanoparticles for Electrochemical Lithium-Ion Storage
(McBean, Coray L.; Wang, Lei; Moronta, Dominic; Scida, Alexis; Li, Luyao; Takeuchi, Esther S.; Takeuchi, Kenneth J.; Marschilok, Amy C.; Wong, Stanislaus S.)
Tag: EC, Li, ret, MAG, NP

[ACS Appl. Energy Mater. 2019080211213, 2019, 7−4833]
Defect Structure and Photovoltaic Characteristics of Internally Stacked CuO/Cu₂O Photoactive Layer Prepared by Electrodeposition and Heating
(Izaki, Masanobu; Fukazawa, Kazuma; Sato, Kenta; Khoo, Pei Loon; Kobayashi, Masakazu; Takeuchi, Akihisa; Uesugi, Kentaro)
Tag: pc, PV, em, VL, SC, ED

[ACS Appl. Energy Mater. 20190802112148, 2019, 7−4865]
Platinum and PtNi Nanoparticle-Supported Multiwalled Carbon Nanotube Electrocatalysts Prepared by One-Pot Pyrolytic Synthesis with an Ionic Liquid
(Yao, Yu; Izumi, Reiko; Tsuda, Tetsuya; Oshima, Yoshifumi; Imanishi, Akihito; Oda, Naoko; Kuwabata, Susumu)
Tag: NT, MWCNT, Ni, C, Pt, O, CNT, NP, IL, ORR, Cat

[ACS Appl. Energy Mater. 20190802112517, 2019, 7−5039]
Influence of a Hole-Transport Layer on Light-Induced Degradation of Mixed Organic–Inorganic Halide Perovskite Solar Cells
(Sekimoto, Takeyuki; Matsui, Taisuke; Nishihara, Takashi; Uchida, Ryusuke; Sekiguchi, Takashi; Negami, Takayuki)
Tag: HAXPES, PE, ETL, IS, PSC, EC, XPS, I, HTL, PS, e-, P, LID

[ACS Appl. Energy Mater. 20190802112638, 2019, 7−5103]
Examination of a Cu-Deficient Layer on Cu(In, Ga)Se₂ Films Fabricated by a Three-Stage Process for Highly Efficient Solar Cells
(Nishimura, Takahito; Nakada, Kazuyoshi; Yamada, Akira)
Tag: VB, PE, EDS, EDX, UV, VBO, PS, TEM, DPC, UPS, e-